Trenbolone Cyclohexylmethylcarbonate CAS:23454-33-3 11-trien-3-one carbonate cyclohexylMethylcarbonate (8CI)

Chiyambi chachidule:
Trenbolone (TRE) ndi steroid protein assimilation hormone yomwe imagwiritsidwa ntchito kwambiri.Ndichochokera ku chemosynthetic chofanana ndi mahomoni aamuna a testosterone pamapangidwe ndi ntchito.Ikhoza kulimbikitsa kaphatikizidwe ka mapuloteni, kuonjezera chilakolako cha chakudya, kuonjezera minofu, kulimbikitsa calcium ndi phosphorous mu minofu ya mafupa, ndipo ingagwiritsidwe ntchito kuchipatala pofuna kuchiza kuperewera kwa zakudya m'thupi ndi kufooka kwa mafupa, komanso ndi mtundu womwe umagwiritsidwa ntchito mobwerezabwereza wa masewera olimbitsa thupi.Gulu bolone cyclohexyl methyl carbonate angagwiritsidwe ntchito ngati kupanga wapakatikati wa gulu Bolone.
Kukonzekera:
Gulu la bromcyclohexyl methyl carbonate limakonzedwa motere:
3G17/3-hydroxy-estradiol-4,9, 11-triene-3-one inasungunuka mu pyridine pa 15 ℃ ndi 0 ℃ pansi pa chipwirikiti ndi mpweya wa nayitrogeni.Sungani kutentha kwapakati pa 0 mpaka 10 digiri Celsius.Pang'onopang'ono onjezani 50ml hexahydrobenzyl chloride Chemicalbook formate, kenaka tenthetsani chisakanizo chonse ku kutentha kozungulira, yambitsani kwa maola 2, kenako ozizira mpaka 0 ° C. Onjezani triethylamine ndikuyambitsa kwa mphindi 30 kuti muwonjezere kutentha kuti mukhale wozungulira ndikutsanulira zomwe zimasakanikirana mumadzi. madzi / ayezi osakaniza.Anachotsedwa ndi methylene chloride, ndipo gawo la organic linatsukidwa ndi madzi kuti asalowerere, zouma ndi sodium sulphate, ndipo zimatuluka nthunzi pansi pa vacuum mpaka zitauma.Chotsaliracho chinasiyanitsidwa ndi chromatography pa silica gel, yopangidwa ndi 4: 1 osakaniza a benzene/ethyl acetate, ndi recrystallized kuchokera isopropyl ether/hexane osakaniza.Chromatography inachitidwanso pa silika gel, eluted ndi osakaniza a benzene/ethyl acetate, ndipo potsiriza recrystallized kuchokera cyclohexane ndi petroleum ether kupeza 1.60g gulu bromcyclohexyl methyl carbonate.Mankhwalawa amawoneka ngati prism sungunuka mu ethanol, ether, benzene, acetone, ndi chloroform, koma osasungunuka m'madzi, kusungunula asidi, ndi lye.