Trenbolone Cyclohexylmethylcarbonate CAS: 23454-33-3 11-trien-3-one carbonate cyclohexylMethylcarbonate (8CI)

A takaice gabatarwa:
Trenbolone (TRE) ne mai yadu amfani steroid protein assimilation hormone.Yana da wani nau'in chemosynthetic mai kama da testosterone na namiji na mutum a cikin tsari da aiki.Yana iya inganta haɓakar furotin, ƙara yawan ci, ƙara tsoka, inganta calcium da phosphorus a cikin nama na kashi, kuma ana iya amfani da shi a asibiti don magance rashin lafiya mai tsanani da kuma osteoporosis, amma kuma shine mafi yawan amfani da nau'in motsa jiki na wasanni.Ƙungiyar bolone cyclohexyl methyl carbonate za a iya amfani da shi azaman tsaka-tsakin roba na rukuni na Bolone.
Shiri:
Rukunin bromcyclohexyl methyl carbonate an shirya kamar haka:
3G17/3-hydroxy-estradiol-4,9, 11-triene-3-daya aka narkar da a pyridine a 15 ℃ da 0 ℃ a karkashin agitation da nitrogen yanayi.Rike zafin jiki tsakanin 0 zuwa 10 digiri Celsius.A hankali ƙara 50ml hexahydrobenzyl chloride Chemicalbook formate, sa'an nan kuma dumama dukan cakuda zuwa yanayin zafin jiki, motsawa na tsawon awanni 2, sa'an nan kuma kwantar da shi zuwa 0 ° C. Ƙara triethylamine da motsawa na minti 30 don tayar da zafin jiki zuwa yanayi kuma zuba cakudawar dauki a cikin cakuda ruwa/kankara.An fitar da shi tare da methylene chloride, kuma tsarin kwayoyin halitta an wanke shi da ruwa zuwa tsaka tsaki, an bushe shi da sodium sulfate, kuma an kwashe shi a karkashin injin har sai ya bushe.An raba ragowar ta hanyar chromatography akan gel silica, wanda aka haɓaka tare da 4: 1 cakuda benzene / ethyl acetate, kuma an sake sake shi daga cakuda isopropyl ether / hexane.An sake yin chromatography akan gel silica, wanda aka haɓaka tare da cakuda benzene / ethyl acetate, kuma a ƙarshe an sake yin recrystallized daga cyclohexane da ether petroleum don samun 1.60g ƙungiyar bromcyclohexyl methyl carbonate.Samfurin yana bayyana azaman mai narkewa a cikin ethanol, ether, benzene, acetone, da chloroform, amma maras narkewa a cikin ruwa, dilute acid, da mafita na lye.